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1 article(s) from Kunz, Anne

Continuous flow synthesis of azobenzenes via Baeyer–Mills reaction

Jan H. Griwatz,
Anne Kunz and
Hermann A. Wegner

Beilstein J. Org. Chem. 2022, 18, 781–787, doi:10.3762/bjoc.18.78

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Scheme 1: Baeyer–Mills reaction of AB (1a) involving nucleophilic attack of aniline (2a) to nitrosobenzene (3...

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Figure 1: Flow setup for optimization of the Baeyer–Mills reaction with aniline (2a) and nitrosobenzene (3). ...

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Figure 2: Optimization of the Baeyer–Mills reaction of nitrosobenzene (3) with aniline (2a) to AB (1a). The n...

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Figure 3: Flow setup after prior optimization with unsubstituted aniline (2a) and nitrosobenzene (3) to AB (1a...

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Scheme 2: Large-scale synthesis of AB 1t from aniline 2t and nitrosobenzene (3) in >99% yield within 3 days.

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Published 30 Jun 2022

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